From kay.gastinger at ntnu.no Fri Feb 2 07:23:39 2018 From: kay.gastinger at ntnu.no (Kay Gastinger) Date: Fri, 2 Feb 2018 12:23:39 +0000 Subject: [labnetwork] Hazardous gas delivery logistics In-Reply-To: <012c01d39ac6$a8c1c670$fa455350$@columbia.edu> References: <012c01d39ac6$a8c1c670$fa455350$@columbia.edu> Message-ID: Dear Nava, I would not trust on the gas company. At least in Norway, the drivers have rather low competence, so take control as soon as the gas comes off the trailer. I would make sure that nobody except your experts are in the area, definitely close the corridors/elevators, nobody travels in an elevator together with the gas. Make sure the bottles are secured against falling off during transport. Be aware they come in different sizes, you might need several sizes of transport devices. We have always 2 of our engineers with oxygen masks (both) connecting the bottles, one works - one checks. Both plan the work together and make a list of steps on how to proceed. If unplanned things happens, stop the work and make a new plan that both agree on. Write it down and follow strictly. If we handle Silane I would also recommend a fire fighter dress. We did not leak check the bottles when they came, as far as I remember. Turn on emergency ventilation under installation. Standard procedure when connecting with leak check etc. store The gas bottles in its cabinets until installation. I assume of course your gas detection system is tested and operational. NI purging is important before connecting. Take care of the ?other end? of the pipes when starting up a new system. I would close the cleanroom and also here the gas detection system should of course be operational. The gas pipes are leak tested? We found after some year out that the welds in our system were not tested with x-rays. That I would really recommend. We tested 10% of the joints and found considerable pits in one of the pipes, that we had to repair later-on which is much more challenging with all the other pipes and dangerous gases around. I hope that helped. Kay -------------------------------------------------------------------------------------------- Kay Gastinger, PhD Director NTNU NanoLab, Chemistry building I / room 122, N-7491 Trondheim Norway tel. +47 / 7359 1490 mob. +47 / 982 83 906 www.ntnu.edu/nanolab -------------------------------------------------------------------------------------------- From: on behalf of Nava Ariel-Sternberg Date: Wednesday, 31 January 2018 at 23:50 To: "labnetwork at mtl.mit.edu" Subject: [labnetwork] Hazardous gas delivery logistics Dear all, I am very happy to say that we are finally gearing up to full operations in the Columbia University clean room (after a long renovation period, inspections, permits etc.). The final stage will be to bring on-line systems that use toxic and other hazardous gases that we do not yet have on site. As we are getting ready to receive those gases, we started discussing what would be the safest way to receive them and the logistics involved. This has brought some interesting questions and I wanted to get some inputs from other facilities. Could you please comment on the toxic gases receiving procedures in your facility? Is the delivery done at special times in the day? Are you securing the cylinder path? (making sure no one is in the corridor/elevator etc.?) Are you performing leak checks when the cylinder arrives to campus? Are staff wearing SCBA when handling the cylinders? When is the transfer point between the gas company and the technical staff of the clean room? Thanks, Nava Nava Ariel-Sternberg, Ph.D. Director of CNI Shared Facilities Columbia University 530 w120th st., NY 10027 Room 1015/MC 8903 Office: 212-854-9927 Cell: 201-562-7600 ? -------------- next part -------------- An HTML attachment was scrubbed... URL: From gcure at email.arizona.edu Fri Feb 2 12:40:17 2018 From: gcure at email.arizona.edu (Cure, Gregg D - (gcure)) Date: Fri, 2 Feb 2018 17:40:17 +0000 Subject: [labnetwork] Astech ATL-100RA manual Message-ID: Hello folks, Would any of you have a PDF mannual for an Astech ATL-100AR RF matching network? Thanks in advance, Gregg Cure` Gregg D. Cure` The University of Arizona Office for Research and Discovery Nano Fabrication and Processing Center 1230 E. Speedway Blvd. ECE104 Rm 209 Tucson, AZ 85721-0104 Office: 520.626.1987 Cell: 520.307.0925 Fax: 520.626.7877 Website: http://mfc.arizona.edu Website: http://research.arizona.edu/ -------------- next part -------------- An HTML attachment was scrubbed... URL: From Vincent.Luciani at nist.gov Fri Feb 2 14:19:02 2018 From: Vincent.Luciani at nist.gov (Luciani, Vincent (Fed)) Date: Fri, 2 Feb 2018 19:19:02 +0000 Subject: [labnetwork] Hazardous gas delivery logistics In-Reply-To: <012c01d39ac6$a8c1c670$fa455350$@columbia.edu> References: <012c01d39ac6$a8c1c670$fa455350$@columbia.edu> Message-ID: Hello Nava, I recommend an inspection checklist and a hand held sniffer before a cylinder is permitted to be unloaded. Perhaps it has changed since my last deep dive into the details but there are ?cradle-to-grave? codes and responsibilities with regard to toxic gasses. Once the cylinder is off the truck the recipient has additional responsibilities with regard to handling that cylinder if it turns out to be a leaker. The vendors have special mobile units to deal with such cylinders but would much rather drop it and leave, making it your problem. Before it gets off the truck, the valve should be visually checked to make sure it is wrapped and protected from weather, no rust or debris in the outlet, that it has the right CGA fitting, the outlet cap is in place, valve neck is not bent etc. etc. etc. and of course that the sniffer does not detect a leak. If it checks out, you allow the driver to unload the cylinder and you can treat it as a known non-leaker and carefully transport it like any other cylinder to its safe location. If it does not check out, you can refuse delivery and thus it is still in the vendor?s ?cradle-to-grave? responsibility and they must deal with it. Vince Vincent K. Luciani NanoFab Manager Center for Nanoscale Science and Technology National Institute of Standards and Technology 100 Bureau Drive, MS 6201 Gaithersburg, MD 20899-6200 USA +1-301-975-2886 From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Nava Ariel-Sternberg Sent: Wednesday, January 31, 2018 2:07 PM To: labnetwork at mtl.mit.edu Subject: [labnetwork] Hazardous gas delivery logistics Dear all, I am very happy to say that we are finally gearing up to full operations in the Columbia University clean room (after a long renovation period, inspections, permits etc.). The final stage will be to bring on-line systems that use toxic and other hazardous gases that we do not yet have on site. As we are getting ready to receive those gases, we started discussing what would be the safest way to receive them and the logistics involved. This has brought some interesting questions and I wanted to get some inputs from other facilities. Could you please comment on the toxic gases receiving procedures in your facility? Is the delivery done at special times in the day? Are you securing the cylinder path? (making sure no one is in the corridor/elevator etc.?) Are you performing leak checks when the cylinder arrives to campus? Are staff wearing SCBA when handling the cylinders? When is the transfer point between the gas company and the technical staff of the clean room? Thanks, Nava Nava Ariel-Sternberg, Ph.D. Director of CNI Shared Facilities Columbia University 530 w120th st., NY 10027 Room 1015/MC 8903 Office: 212-854-9927 Cell: 201-562-7600 ? -------------- next part -------------- An HTML attachment was scrubbed... URL: From schweig at umich.edu Sat Feb 3 06:42:53 2018 From: schweig at umich.edu (Dennis Schweiger) Date: Sat, 3 Feb 2018 06:42:53 -0500 Subject: [labnetwork] Hazardous gas delivery logistics Message-ID: Nava, good morning. Here at the University of Michigan/LNF our gas vendor has access to the chemical dock delivery for our lab (they deliver at 4:30-5 in the morning) and the normal gases (N2, Ar, He, O2, H2, CH4, etc.) are delivered by them. When our staff arrive around 7, those cylinders will be moved to their proper storage location. The delivery person will also pick up the empties at the same time. For all of the HPM materials (SiH4, NH3, NF3, AsH3, PH3, BCl3, Cl2, etc), we've "right sized" both the cylinders, and the fills, so that we have a cylinder change out cadence of 12-18 months. This means that the physically largest HPM cylinder we have in our site is one of the Silanes. It's about 9" diameter and 24" tall. All of the HPM cylinders are shipped common carrier to our building dock, however our receiving crew for the building will call me as soon as they arrive, and either myself, or another individual, will go pick them up. The distance between that dock, and our controlled service aisle is about 125' through a seldomly used building corridor. We use all DISS cylinder valves on our HPM's, they're shipped blanked off, and then when the cylinder goes into one of the gas storage rooms of our fab, those new "full" cylinders are stored in the lower half of the gas cabinet that houses the online cylinder. We'll wear SCBA only when we break the cylinder valve cap to do a change out. So far, this procedure (in place since 2008) has worked well for us, and has not created any issues with either getting the gas in a timely fashion, or unnecessarily exposing the building occupants to an exposure risk. Dennis Schweiger Facilities Manager University of Michigan/LNF 734.647.2055 Ofc On Wed, Jan 31, 2018 at 2:06 PM, Nava Ariel-Sternberg wrote: > Dear all, > > > > I am very happy to say that we are finally gearing up to full operations > in the Columbia University clean room (after a long renovation period, > inspections, permits etc.). The final stage will be to bring on-line > systems that use toxic and other hazardous gases that we do not yet have on > site. As we are getting ready to receive those gases, we started discussing > what would be the safest way to receive them and the logistics involved. > This has brought some interesting questions and I wanted to get some inputs > from other facilities. > > > > Could you please comment on the toxic gases receiving procedures in your > facility? Is the delivery done at special times in the day? Are you > securing the cylinder path? (making sure no one is in the corridor/elevator > etc.?) Are you performing leak checks when the cylinder arrives to campus? > Are staff wearing SCBA when handling the cylinders? When is the transfer > point between the gas company and the technical staff of the clean room? > > > > Thanks, > > Nava > > > > > > Nava Ariel-Sternberg, Ph.D. > > Director of CNI Shared Facilities > > Columbia University > > 530 w120th st., NY 10027 > > Room 1015/MC 8903 > > Office: 212-854-9927 <(212)%20854-9927> > > Cell: 201-562-7600 <(201)%20562-7600> > > > > ? > > > > _______________________________________________ > labnetwork mailing list > labnetwork at mtl.mit.edu > https://mtl.mit.edu/mailman/listinfo.cgi/labnetwork > > -------------- next part -------------- An HTML attachment was scrubbed... URL: From eabelev at pitt.edu Mon Feb 5 11:33:38 2018 From: eabelev at pitt.edu (Abelev, Esta) Date: Mon, 5 Feb 2018 16:33:38 +0000 Subject: [labnetwork] Ge2Sb2Te5 deposition and annealing Message-ID: Dear Colleagues, I would like to ask about deposition and annealing of Ge2Sb2Te5. The sputtering system we use for Ge2Sb2Te5 deposition is without load lock, the smell after depositing is horrible but my main concerns is regarding toxicity. Do you know if those materials/odor toxic? In addition, the group wants to anneal those samples in RTA at low temp (below 200C) after the deposition, I am concerns about contaminations? Please comment. Thank you, Esta ----------------------- Esta Abelev, PhD Technical Director, Petersen Institute of NanoScience and Engineering University of Pittsburgh | 3700 O'Hara Street | 636| Pittsburgh, PA 15261 412-383-4096 | eabelev at pitt.edu | nano.pitt.edu -------------- next part -------------- An HTML attachment was scrubbed... URL: From myoung6 at nd.edu Mon Feb 5 16:58:45 2018 From: myoung6 at nd.edu (Michael Young) Date: Mon, 5 Feb 2018 16:58:45 -0500 Subject: [labnetwork] Ge2Sb2Te5 deposition and annealing In-Reply-To: References: Message-ID: <56ae934b-75c3-ad22-c956-8f1fdad8bb9d@nd.edu> An HTML attachment was scrubbed... URL: From bill_flounders at berkeley.edu Mon Feb 5 16:58:28 2018 From: bill_flounders at berkeley.edu (A. William (Bill) FLOUNDERS) Date: Mon, 5 Feb 2018 13:58:28 -0800 Subject: [labnetwork] Ge2Sb2Te5 deposition and annealing In-Reply-To: References: Message-ID: Esta Abelev, Consult with your campus EH&S. Tellurium is known for its stench (same family as sulfur) and exposure to miniscule amounts results in a condition known as tellurium breath. Both tellurium and antimony are considered mildly toxic and have defined threshold exposure limits. Multiple pump/purge cycles are recommended prior to opening your chamber. As with any metals, avoid any operations that would generate particulates / dust. Bill Flounders UC Berkeley On Mon, Feb 5, 2018 at 8:33 AM, Abelev, Esta wrote: > Dear Colleagues, > > > > I would like to ask about deposition and annealing of Ge2Sb2Te5. > > The sputtering system we use for Ge2Sb2Te5 deposition is without load > lock, the smell after depositing is horrible but my main concerns is > regarding toxicity. Do you know if those materials/odor toxic? > > In addition, the group wants to anneal those samples in RTA at low temp > (below 200C) after the deposition, I am concerns about contaminations? > Please comment. > > > > Thank you, Esta > > > > ----------------------- > > *Esta Abelev, PhD* > > Technical Director, Petersen Institute of NanoScience and Engineering > > University of Pittsburgh | 3700 O?Hara Street | 636| Pittsburgh, PA 15261 > > 412-383-4096 <(412)%20383-4096> | eabelev at pitt.edu | nano.pitt.edu > > > > > > > _______________________________________________ > labnetwork mailing list > labnetwork at mtl.mit.edu > https://mtl.mit.edu/mailman/listinfo.cgi/labnetwork > > -------------- next part -------------- An HTML attachment was scrubbed... URL: From miller at purdue.edu Tue Feb 6 15:54:31 2018 From: miller at purdue.edu (Miller, Timothy J) Date: Tue, 6 Feb 2018 20:54:31 +0000 Subject: [labnetwork] Dicing Indium Antimonide? Message-ID: Subject line says it all - does anyone have experience dicing Indium Antimonide? Timothy J. Miller Purdue University Birck Nanotechnology Center 1205 West State Street West Lafayette, IN 47907-2057 765-427-4712 -------------- next part -------------- An HTML attachment was scrubbed... URL: From nclay at upenn.edu Tue Feb 6 21:32:51 2018 From: nclay at upenn.edu (Noah Clay) Date: Tue, 6 Feb 2018 21:32:51 -0500 Subject: [labnetwork] Dicing Indium Antimonide? In-Reply-To: References: Message-ID: <61F80174-E715-426F-A8BA-157222127B22@upenn.edu> Tim, I worked with this material in industry. We diced it on a Loomis LSD-150, in notch and break mode. Scribe and break mode generates excessive dust -> no go...and we couldn?t saw it without capturing the waste water - and, besides, the saw would be contaminated. While scribing, I?d advise your PI?s researchers to wear a face mask (covering mouth/nose), double-glove and wipe-down the machine as well as nearby table surfaces after each use (alpha wipes and IPA). The dust will be insignificant, so it can be disposed of in the regular trash along with their outer gloves. Any wafer fragments that are left over should be placed in a III-V waste container that your EHS will dispose of when full. You could take things to the next level with swab or wipe tests (using an industrial hygiene company) of nearby table surfaces after 6-12 months to benchmark contamination levels. Best, Noah Sent from my iPhone > On Feb 6, 2018, at 15:54, Miller, Timothy J wrote: > > Subject line says it all ? does anyone have experience dicing Indium Antimonide? > > Timothy J. Miller > Purdue University > Birck Nanotechnology Center > 1205 West State Street > West Lafayette, IN 47907-2057 > 765-427-4712 > > _______________________________________________ > labnetwork mailing list > labnetwork at mtl.mit.edu > https://mtl.mit.edu/mailman/listinfo.cgi/labnetwork -------------- next part -------------- An HTML attachment was scrubbed... URL: From mhofheins at unm.edu Wed Feb 7 10:28:43 2018 From: mhofheins at unm.edu (Mark Hofheins) Date: Wed, 7 Feb 2018 15:28:43 +0000 Subject: [labnetwork] Molybdenum sputtering Message-ID: Good Morning All, I have a customer that wants to sputter Mo. What is a recommended wattage and what types of contamination do I need to be concerned with? Mark Hofheins mhofheins at unm.edu 505-710-3527 Micro Electronics Technician Manufacturing Engineering University of New Mexico MTTC 800 Bradbury S.E. Suit 235 Albuquerque, New Mexico 87106-4346 -------------- next part -------------- An HTML attachment was scrubbed... URL: From mhofheins at unm.edu Fri Feb 9 12:55:25 2018 From: mhofheins at unm.edu (Mark Hofheins) Date: Fri, 9 Feb 2018 17:55:25 +0000 Subject: [labnetwork] ITO and N-Hexane use and handling Message-ID: Good Friday to All, My Director has asked me to inquire on how other universities handle ITO and N-Hexane. What do they use for ventilation and scrubbing for these chemicals? How are these stored? What PPE is used? Please let me know and thank you, Mark Hofheins mhofheins at unm.edu 505-710-3527 Micro Electronics Technician Manufacturing Engineering University of New Mexico MTTC 800 Bradbury S.E. Suit 235 Albuquerque, New Mexico 87106-4346 -------------- next part -------------- An HTML attachment was scrubbed... URL: From khbeis at uw.edu Fri Feb 9 19:18:55 2018 From: khbeis at uw.edu (Michael Khbeis) Date: Fri, 9 Feb 2018 16:18:55 -0800 Subject: [labnetwork] Best practices for chemical storage, cross contamination, conservation Message-ID: <8E6984FA-E127-4CEF-8E36-B857AC6FBB52@uw.edu> Dear Colleagues, We have many users avoiding shared baths for things like RCA, Piranha, and even developers because they worry about cross-contamination (and rightfully so with random things floating in the baths on a fairly regular basis). However, this has led to numerous users pouring resealable, food grade containers, that subsequently leave them cluttered on our wet process station work surfaces for up to several weeks. This of course is not an acceptable solution but prohibiting this behavior will result in a massive waste of otherwise perfectly good chemicals. So we have a challenge of balancing process integrity, safety, and chemical economy. We are looking for better temporary storage solutions that would allow transport of containers to chemical cabinets, but I am curious how other sites have resolved or administered this issue. Gratefully, Dr. Michael Khbeis Director, Washington Nanofabrication Facility (WNF) National Nanotechnology Coordinated Infrastructure (NNCI) University of Washington Fluke Hall, Box 352143 (O) 206.543.5101 (F) 206.221.1681 (C) 443.254.5192 khbeis at uw.edu www.wnf.washington.edu/ -------------- next part -------------- An HTML attachment was scrubbed... URL: -------------- next part -------------- A non-text attachment was scrubbed... Name: smime.p7s Type: application/pkcs7-signature Size: 1350 bytes Desc: not available URL: From fouad.karouta at anu.edu.au Sun Feb 11 17:56:51 2018 From: fouad.karouta at anu.edu.au (Fouad Karouta) Date: Sun, 11 Feb 2018 22:56:51 +0000 Subject: [labnetwork] Best practices for chemical storage, cross contamination, conservation In-Reply-To: <8E6984FA-E127-4CEF-8E36-B857AC6FBB52@uw.edu> References: <8E6984FA-E127-4CEF-8E36-B857AC6FBB52@uw.edu> Message-ID: Hi Michael, Working with chemicals is a delicate matter and unless you have clear rules about what can be used in shared baths and what cannot. However this description may still be misinterpreted by users. I am not sure if you have users using wet etchants for wafer batches (25x). If users are only using one wafer to smaller pieces at one time you can limit the amount of chemicals used by having adequate containers to use a limited amount of chemical even with a one 4" wafer (beaker with 11 cm diameter and 5-6 cm edge height). For HF I tend to get regular size containers then get it machined in workshop to reduce the height. Each user makes his solution and use it then dispose of it upon the rules (neutralize, etc.). You may consider the following: * To avoid having every user preparing upfront those chemicals and putting a pressure on the storage area, you may consider having one container of each regularly used solution prepared and topped up by your staff, this can go for RCA, HF dilutions, etc. * A remark about piranha solution though I suppose the purpose is just cleaning the wafer but H2O2 is unstable in acidic solution and you should consider how long such a solution can be used. Regards, Fouad Karouta ************************************* Manager ANFF ACT Node Australian National Fabrication Facility Research School of Physics and Engineering L. Huxley Building (#56), Mills Road, Room 4.02 Australian National University ACT 0200, Canberra, Australia Tel: + 61 2 6125 7174 Mob: + 61 451 046 412 Email: fouad.karouta at anu.edu.au http://anff-act.anu.edu.au/ From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Michael Khbeis Sent: Saturday, 10 February 2018 11:19 AM To: labnetwork at mtl.mit.edu Subject: [labnetwork] Best practices for chemical storage, cross contamination, conservation Dear Colleagues, We have many users avoiding shared baths for things like RCA, Piranha, and even developers because they worry about cross-contamination (and rightfully so with random things floating in the baths on a fairly regular basis). However, this has led to numerous users pouring resealable, food grade containers, that subsequently leave them cluttered on our wet process station work surfaces for up to several weeks. This of course is not an acceptable solution but prohibiting this behavior will result in a massive waste of otherwise perfectly good chemicals. So we have a challenge of balancing process integrity, safety, and chemical economy. We are looking for better temporary storage solutions that would allow transport of containers to chemical cabinets, but I am curious how other sites have resolved or administered this issue. Gratefully, Dr. Michael Khbeis Director, Washington Nanofabrication Facility (WNF) National Nanotechnology Coordinated Infrastructure (NNCI) University of Washington Fluke Hall, Box 352143 (O) 206.543.5101 (F) 206.221.1681 (C) 443.254.5192 khbeis at uw.edu www.wnf.washington.edu/ -------------- next part -------------- An HTML attachment was scrubbed... URL: From Vincent.Luciani at nist.gov Mon Feb 12 09:17:47 2018 From: Vincent.Luciani at nist.gov (Luciani, Vincent (Fed)) Date: Mon, 12 Feb 2018 14:17:47 +0000 Subject: [labnetwork] Best practices for chemical storage, cross contamination, conservation In-Reply-To: <8E6984FA-E127-4CEF-8E36-B857AC6FBB52@uw.edu> References: <8E6984FA-E127-4CEF-8E36-B857AC6FBB52@uw.edu> Message-ID: Good Morning Michael, I can't say we have the problem solved but we have made some headway. This is what we have done to date: We purchased single wafer piranha and RCA spray clean tools. We are just about to wrap up an oxide integrity study comparing it to immersion RCA. It looks encouraging. Works with whole wafers (75 mm - 200 mm). This saves chemicals and manual pouring and handling of waste. Every Friday evening at about 11 PM, we clear the benches. Most people know this so there is not much to clean up. During the week, any beakers that are not labelled properly are removed as soon as we find them. I am still not happy with our resist and developer handling management. Still very manual with users having direct access to gallon containers. There is a session dedicated to lithography materials management in this year's https://ugim.nano.upenn.edu/ . I encourage anyone with something to contribute to send in an abstract. If the upload is not functional yet, send it to me. Best, Vince From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Michael Khbeis Sent: Friday, February 09, 2018 7:19 PM To: labnetwork at mtl.mit.edu Subject: [labnetwork] Best practices for chemical storage, cross contamination, conservation Dear Colleagues, We have many users avoiding shared baths for things like RCA, Piranha, and even developers because they worry about cross-contamination (and rightfully so with random things floating in the baths on a fairly regular basis). However, this has led to numerous users pouring resealable, food grade containers, that subsequently leave them cluttered on our wet process station work surfaces for up to several weeks. This of course is not an acceptable solution but prohibiting this behavior will result in a massive waste of otherwise perfectly good chemicals. So we have a challenge of balancing process integrity, safety, and chemical economy. We are looking for better temporary storage solutions that would allow transport of containers to chemical cabinets, but I am curious how other sites have resolved or administered this issue. Gratefully, Dr. Michael Khbeis Director, Washington Nanofabrication Facility (WNF) National Nanotechnology Coordinated Infrastructure (NNCI) University of Washington Fluke Hall, Box 352143 (O) 206.543.5101 (F) 206.221.1681 (C) 443.254.5192 khbeis at uw.edu www.wnf.washington.edu/ -------------- next part -------------- An HTML attachment was scrubbed... URL: From julia.aebersold at louisville.edu Mon Feb 12 11:14:54 2018 From: julia.aebersold at louisville.edu (Aebersold,Julia W.) Date: Mon, 12 Feb 2018 16:14:54 +0000 Subject: [labnetwork] Best practices for chemical storage, cross contamination, conservation In-Reply-To: References: <8E6984FA-E127-4CEF-8E36-B857AC6FBB52@uw.edu> Message-ID: We have our users prepare new RCA and Piranha baths for their applications for their stability varies over time. We tried baths for developers, but it gave us varying developer times for our clients. So we have dedicated containers for developers and clients user new developer for each process. We also found that it reduced our overall developer usage. For HF we have a dedicated BOE bath that gets changed on a periodic basis. If folks need 49% HF then they make use specific what we need. I prefer not to keep a bath of that sort on hand due to infrequent usage and its danger factor. Cheers! Julia Aebersold Manager, Micro/Nano Technology Center University of Louisville Shumaker Research Building, Room 233 2210 South Brook Street Louisville, KY 40292 (502) 852-1572 http://louisville.edu/micronano/ From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Fouad Karouta Sent: Sunday, February 11, 2018 5:57 PM To: Michael Khbeis ; labnetwork at mtl.mit.edu Subject: Re: [labnetwork] Best practices for chemical storage, cross contamination, conservation Hi Michael, Working with chemicals is a delicate matter and unless you have clear rules about what can be used in shared baths and what cannot. However this description may still be misinterpreted by users. I am not sure if you have users using wet etchants for wafer batches (25x). If users are only using one wafer to smaller pieces at one time you can limit the amount of chemicals used by having adequate containers to use a limited amount of chemical even with a one 4" wafer (beaker with 11 cm diameter and 5-6 cm edge height). For HF I tend to get regular size containers then get it machined in workshop to reduce the height. Each user makes his solution and use it then dispose of it upon the rules (neutralize, etc.). You may consider the following: * To avoid having every user preparing upfront those chemicals and putting a pressure on the storage area, you may consider having one container of each regularly used solution prepared and topped up by your staff, this can go for RCA, HF dilutions, etc. * A remark about piranha solution though I suppose the purpose is just cleaning the wafer but H2O2 is unstable in acidic solution and you should consider how long such a solution can be used. Regards, Fouad Karouta ************************************* Manager ANFF ACT Node Australian National Fabrication Facility Research School of Physics and Engineering L. Huxley Building (#56), Mills Road, Room 4.02 Australian National University ACT 0200, Canberra, Australia Tel: + 61 2 6125 7174 Mob: + 61 451 046 412 Email: fouad.karouta at anu.edu.au http://anff-act.anu.edu.au/ From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Michael Khbeis Sent: Saturday, 10 February 2018 11:19 AM To: labnetwork at mtl.mit.edu Subject: [labnetwork] Best practices for chemical storage, cross contamination, conservation Dear Colleagues, We have many users avoiding shared baths for things like RCA, Piranha, and even developers because they worry about cross-contamination (and rightfully so with random things floating in the baths on a fairly regular basis). However, this has led to numerous users pouring resealable, food grade containers, that subsequently leave them cluttered on our wet process station work surfaces for up to several weeks. This of course is not an acceptable solution but prohibiting this behavior will result in a massive waste of otherwise perfectly good chemicals. So we have a challenge of balancing process integrity, safety, and chemical economy. We are looking for better temporary storage solutions that would allow transport of containers to chemical cabinets, but I am curious how other sites have resolved or administered this issue. Gratefully, Dr. Michael Khbeis Director, Washington Nanofabrication Facility (WNF) National Nanotechnology Coordinated Infrastructure (NNCI) University of Washington Fluke Hall, Box 352143 (O) 206.543.5101 (F) 206.221.1681 (C) 443.254.5192 khbeis at uw.edu www.wnf.washington.edu/ -------------- next part -------------- An HTML attachment was scrubbed... URL: From ida.noddeland at ntnu.no Tue Feb 13 05:53:45 2018 From: ida.noddeland at ntnu.no (Ida Noddeland) Date: Tue, 13 Feb 2018 10:53:45 +0000 Subject: [labnetwork] Vacant engineer position at Tyndall, Ireland Message-ID: <9fb678b65d1547dd979afd3063372146@it-ex11.win.ntnu.no> Dear all, There is a vacancy for a senior maintenance engineer at Tyndall National Institute in Cork, Ireland. Please share this link with anyone who may be interested! http://careers.tyndall.ie/vacancies/senior-maintenance-engineer-senior-technical-officer Best regards Ida Noddeland Head of Laboratory NTNU NanoLab Sem S?lands vei 14, K1-123 7491 Trondheim +47 412 88 808 www.ntnu.no/nano -------------- next part -------------- An HTML attachment was scrubbed... URL: From gilheart at rice.edu Tue Feb 13 17:13:19 2018 From: gilheart at rice.edu (Tim Gilheart) Date: Tue, 13 Feb 2018 16:13:19 -0600 Subject: [labnetwork] Research Scientist position in Rice U. cleanroom Message-ID: <6161DF83-F15E-45FB-B5B0-CB8227624C36@rice.edu> Greetings colleagues, We have an opening on the cleanroom team with the Shared Equipment Authority (SEA) at Rice University. More information about the position may be found here: https://jobs.rice.edu/postings/12671 The cleanroom at Rice is part of the SEA, a larger umbrella organization under the Vice Provost for Research, that administers a number of shared core labs (electron microscopy, nanofab cleanroom, NMR, mass spec, optical microscopy, XRD, etc) located throughout the university. This position is part of the SEA's collegial team of scientists that support research efforts from the schools of engineering and natural sciences. More information about the SEA can be found on our website: https://sea.rice.edu/ Rice is still accepting applications for this position, so if you know a good candidate, please pass this information along to them. This is an exciting time to join our team, as we are scheduled to move to our new facility in August. With the move, we are replacing some aging workhorse tools, adding altogether new capabilities, and increasing our facility size. Interested candidates are welcome to contact me directly with any questions. Thanks for your time and consideration, -- Tim Gilheart, Ph.D. Research Scientist - Nanofabrication Clean Room Manager, Shared Equipment Authority (SEA), Rice University Cell: 832-341-5488 | Office: 713-348-3159 | gilheart at rice.edu -------------- next part -------------- An HTML attachment was scrubbed... URL: From julia.aebersold at louisville.edu Fri Feb 16 13:53:11 2018 From: julia.aebersold at louisville.edu (Aebersold,Julia W.) Date: Fri, 16 Feb 2018 18:53:11 +0000 Subject: [labnetwork] Open Position - Senior Micro/Nano Technology Process Engineer Message-ID: Hello everyone! We have an open Process Engineering position in the Micro/Nano technology Center at the University of Louisville. Please see the link below for details. https://www.higheredjobs.com/institution/details.cfm?JobCode=176653413&Title=Senior%20Micro%2FNanoTechnology%20Process%20Engineer%20%28Job%20Id%3A%2034550%29&aID=7137 Cheers! Julia Aebersold Manager, Micro/Nano Technology Center University of Louisville Shumaker Research Building, Room 233 2210 South Brook Street Louisville, KY 40292 (502) 852-1572 http://louisville.edu/micronano/ -------------- next part -------------- An HTML attachment was scrubbed... URL: From Vincent.Luciani at nist.gov Fri Feb 16 15:48:31 2018 From: Vincent.Luciani at nist.gov (Luciani, Vincent (Fed)) Date: Fri, 16 Feb 2018 20:48:31 +0000 Subject: [labnetwork] Oxford ICP helium backside cooling performance Message-ID: Hello All, We have 2 Oxford Plasmalab 100 ICP etch tools that are heavily used. 100 mm wafers are the most popular. I am sure I discussed with many of you the trials and tribulations about these tools. My question is about a yur experiences and lessons learned with regard to keeping the helium leak rate from underneath the wafer under control. I am trying to get a general idea of what is typical and how we are doing compared to that. We have several users that utilize the cryonic etching capability of our tools so the helium cooling is very important. For those using the tool at -100 C, we find that 8 sccm is too high and users request repair. We generally try to keep the leak rate < 5 sccm at all time but find this difficult to do with the variety of substrates and etch recipes. We made some progress by ordering specially made quartz discs with a cutout for the wafer flat for better wafer positioning. I am happy to share the dwg if anyone would like it. What is your experience? What leak rate do you find tolerable and at what leak rate do you shut the tool down. Any tricks you can share? Thanks, Vince Vincent K. Luciani NanoFab Manager Center for Nanoscale Science and Technology National Institute of Standards and Technology 100 Bureau Drive, MS 6201 Gaithersburg, MD 20899-6200 USA +1-301-975-2886 -------------- next part -------------- An HTML attachment was scrubbed... URL: From kmcpeak at lsu.edu Fri Feb 16 17:42:53 2018 From: kmcpeak at lsu.edu (Kevin McPeak) Date: Fri, 16 Feb 2018 16:42:53 -0600 Subject: [labnetwork] Open Position - LSU Cleanroom Manager Message-ID: Dear Colleagues, I am excited to announce an open position for a cleanroom manager here at Louisiana State University in Baton Rouge, LA. Please visit the link below for details. https://lsu.wd1.myworkdayjobs.com/LSU/job/LSU---Baton-Rouge/Research-Associate-5_R00020670-1 If you know of potential candidates please pass this along. If you are interested in learning more about the facility don't hesitate to email me offline. Regards, Kevin -- Kevin M. McPeak Assistant Professor Louisiana State University Dept. of Chemical Engineering 110 Chemical Engineering Bldg Room 324 S. Stadium Drive Baton Rouge, LA 70803 email: kmcpeak at lsu.edu phone: 225-578-0058 From km at abeamtech.com Sat Feb 17 01:22:17 2018 From: km at abeamtech.com (Keiko Munechika aBeam) Date: Fri, 16 Feb 2018 22:22:17 -0800 Subject: [labnetwork] Open positions in Nanofabrication Message-ID: <014201d3a7b7$a8a66fd0$f9f34f70$@abeamtech.com> Dear all, Our company has immediate open positions for Nanofabrication Engineer and Nanooptics Scientist. We are located in Hayward, CA and looking for a good candidate at MS level or PhD who would like to continue to do nanofabrication. If you are interested, please contact me off line @ km at abeamtech.com . Also, if you know of any potential candidate for the positions, please pass it along. Many thanks, Keiko Keiko Munechika, Ph.D. Manager, Nanofabrication aBeam Technologies, Inc. Hayward, CA, USA km at abeamtech.com 1-(360)-402-4112 -------------- next part -------------- An HTML attachment was scrubbed... URL: -------------- next part -------------- A non-text attachment was scrubbed... Name: image003.jpg Type: image/jpeg Size: 2028 bytes Desc: not available URL: -------------- next part -------------- A non-text attachment was scrubbed... Name: Job Description for Nanofabrication Engineer.docx.pdf Type: application/pdf Size: 280223 bytes Desc: not available URL: -------------- next part -------------- A non-text attachment was scrubbed... Name: Position Nanooptics aBeam 0118.docx.pdf Type: application/pdf Size: 280189 bytes Desc: not available URL: From smithanair82 at gmail.com Mon Feb 19 06:58:34 2018 From: smithanair82 at gmail.com (smitha nair) Date: Mon, 19 Feb 2018 17:28:34 +0530 Subject: [labnetwork] Oxford ICP helium backside cooling performance In-Reply-To: References: Message-ID: Hello Vincent, We have two Oxford ICP RIE tools (No cryo cooling). On both the tools we face issues with the Helium leak. Most of our users have smaller sample sizes (manually cut), so we use cool grease to stick them on the carrier wafer. The helium flow range acceptable is < 8sccm in these tools and we do not accept anything beyond 10sccm. We address the issue by an open chamber clean as most of the times we end up having cool grease on the chuck. Also if carrier wafer edges are rough or pin holes present, leak is high and we would change the carrier wafer. As you mentioned, is it possible to share the dwg file we could also give a try with quartz wafers. It would be great to know if these issues are more common to Oxford tool or is it general? Regards Smitha Nair Technology Manager National Nanofabrication Centre (NNFC), Centre for Nano Science and Engineering (CeNSE), Indian Institute of Science (IISc), Bangalore-560012. On Sat, Feb 17, 2018 at 2:18 AM, Luciani, Vincent (Fed) < Vincent.Luciani at nist.gov> wrote: > Hello All, > > > > We have 2 Oxford Plasmalab 100 ICP etch tools that are heavily used. 100 > mm wafers are the most popular. I am sure I discussed with many of you the > trials and tribulations about these tools. My question is about a yur > experiences and lessons learned with regard to keeping the helium leak rate > from underneath the wafer under control. I am trying to get a general idea > of what is typical and how we are doing compared to that. We have several > users that utilize the cryonic etching capability of our tools so the > helium cooling is very important. For those using the tool at -100 C, we > find that 8 sccm is too high and users request repair. We generally try to > keep the leak rate < 5 sccm at all time but find this difficult to do with > the variety of substrates and etch recipes. We made some progress by > ordering specially made quartz discs with a cutout for the wafer flat for > better wafer positioning. I am happy to share the dwg if anyone would like > it. > > > > What is your experience? What leak rate do you find tolerable and at what > leak rate do you shut the tool down. Any tricks you can share? > > > > > > Thanks, > > Vince > > > > > > Vincent K. Luciani > > NanoFab Manager > > Center for Nanoscale Science and Technology > > National Institute of Standards and Technology > > 100 Bureau Drive, MS 6201 > > Gaithersburg, MD 20899-6200 USA > > +1-301-975-2886 > > > > > > > > > > > > _______________________________________________ > labnetwork mailing list > labnetwork at mtl.mit.edu > https://mtl.mit.edu/mailman/listinfo.cgi/labnetwork > > -------------- next part -------------- An HTML attachment was scrubbed... URL: From ahad.syed at kaust.edu.sa Mon Feb 19 07:11:26 2018 From: ahad.syed at kaust.edu.sa (Ahad Syed) Date: Mon, 19 Feb 2018 12:11:26 +0000 Subject: [labnetwork] Cleanroom Staff Scientist Position at KAUST Message-ID: <1519042286420.56240@kaust.edu.sa> Dear Colleagues, The Nanofabrication Core Lab (NCL) at KAUST has an open permanent position for a Staff Scientist to work in the Cleanroom and the Micro-Fluidics Lab. Please visit the links below for details https://jobs.kaust.edu.sa/TGWebHost/jobdetails.aspx?SID=%5eRfrlBjD8WuAMKlLHw6rECsgef0YYYI3kxzswWkrIk3gWGzOUBYvAa93KYGYinny5&jobId=629038&type=search&JobReqLang=1&recordstart=1&JobSiteId=5182&JobSiteInfo=629038_5182&GQId=0 https://www.linkedin.com/jobs/view/579573957/ Built on the shores of the Red Sea, KAUST is a graduate level university focused on science and technology. The NCL is a part of the KAUST Core Labs, an organization which reports to the Vice-President of Research and whose mission is to provide state-of-the-art facilities, training and services to the KAUST research community, collaborators and industrial partners. The NCL Cleanroom has 2000sqm of class 100 cleanroom space and is fitted with the latest equipment for micro and nanofabrication. Our latest acquisition is a JEOL JBX-6300FX which has a proven capability to print reliable structures down to 7nm. More information about the NCL and its capabilities can be found at https://corelabs.kaust.edu.sa/nanofabrication/ We offer competitive tax-free salary and outstanding work, living and recreational conditions. The University working language is English and we have an Internal English School (International Baccalaureate) for children on-campus (free of cost). Accommodation (fully-furnished) is provided on-campus. Please pass this information along to any potential candidates. And if you are interested to learn more about the position or the facility, please don't hesitate to email me offline. Thank you, Ahad -- ?Nanofabrication Core Lab 4700 King Abdullah University of Science and Technology 0250-WS02 Building 3, Thuwal 23955-6900, Kingdom of Saudi Arabia Tel:+966 12 808 2348 Visit The Core Labs ________________________________ This message and its contents including attachments are intended solely for the original recipient. If you are not the intended recipient or have received this message in error, please notify me immediately and delete this message from your computer system. Any unauthorized use or distribution is prohibited. Please consider the environment before printing this email. -------------- next part -------------- An HTML attachment was scrubbed... URL: From julia.aebersold at louisville.edu Mon Feb 19 10:46:58 2018 From: julia.aebersold at louisville.edu (Aebersold,Julia W.) Date: Mon, 19 Feb 2018 15:46:58 +0000 Subject: [labnetwork] Oxford ICP helium backside cooling performance In-Reply-To: References: Message-ID: We emphasize a very clean backside before processing is performed. Also, if processing has been performed prior to etching on the wafer then it can incur deformational stress that just makes it hard to sit on the chuck without an elevated leak up rate. We also change the chuck o-rings when the rate starts to climb and perform O2 chamber cleans on a regular basis. Cheers! Julia Aebersold Manager, Micro/Nano Technology Center University of Louisville Shumaker Research Building, Room 233 2210 South Brook Street Louisville, KY 40292 (502) 852-1572 http://louisville.edu/micronano/ From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Luciani, Vincent (Fed) Sent: Friday, February 16, 2018 3:49 PM To: labnetwork at mtl.mit.edu Subject: [labnetwork] Oxford ICP helium backside cooling performance Hello All, We have 2 Oxford Plasmalab 100 ICP etch tools that are heavily used. 100 mm wafers are the most popular. I am sure I discussed with many of you the trials and tribulations about these tools. My question is about a yur experiences and lessons learned with regard to keeping the helium leak rate from underneath the wafer under control. I am trying to get a general idea of what is typical and how we are doing compared to that. We have several users that utilize the cryonic etching capability of our tools so the helium cooling is very important. For those using the tool at -100 C, we find that 8 sccm is too high and users request repair. We generally try to keep the leak rate < 5 sccm at all time but find this difficult to do with the variety of substrates and etch recipes. We made some progress by ordering specially made quartz discs with a cutout for the wafer flat for better wafer positioning. I am happy to share the dwg if anyone would like it. What is your experience? What leak rate do you find tolerable and at what leak rate do you shut the tool down. Any tricks you can share? Thanks, Vince Vincent K. Luciani NanoFab Manager Center for Nanoscale Science and Technology National Institute of Standards and Technology 100 Bureau Drive, MS 6201 Gaithersburg, MD 20899-6200 USA +1-301-975-2886 -------------- next part -------------- An HTML attachment was scrubbed... URL: From mcwilliamss at mail.smu.edu Mon Feb 19 12:38:42 2018 From: mcwilliamss at mail.smu.edu (McWilliams, Scott) Date: Mon, 19 Feb 2018 17:38:42 +0000 Subject: [labnetwork] Technics PlanarEtch IIA/B Message-ID: Hello All, Has anyone used the table top Technics PlanarEtch IIA/B for oxide and/or nitride deposition? I understand I can get a deposition module to convert from etch mode to deposition mode. I would appreciate any input on film quality, ease of use, etc. Also, if know where I can get the deposition module, please let me know. Thanks, Scott -------------- next part -------------- An HTML attachment was scrubbed... URL: From fouad.karouta at anu.edu.au Mon Feb 19 15:39:52 2018 From: fouad.karouta at anu.edu.au (Fouad Karouta) Date: Mon, 19 Feb 2018 20:39:52 +0000 Subject: [labnetwork] Oxford ICP helium backside cooling performance In-Reply-To: References: , Message-ID: <81E93B8D-F8B7-4F63-A528-07EE947FAF27@anu.edu.au> Hi all, Adding to what others mentioned I lie to add: We use dedicated 4? Si wafers as carrier trays when etching small piers that are fixed with Dow Corning 340 heat sink paste, we ask the users to limit the paste to sample area iso it is not exposed directly to the plasma. About the He leak it was less than 2 sccm. If wafer tray or quartz clamp has a chip the He flow may increase so wafer trays should be exempt of chipping. If quartz clamp is damaged it needs replacement. Note the wafer tray should be a good thermal conductor otherwise sample temperature may go much higher than electrode temperature especially with high ICP / RF powers. Regards Fouad Karouta ANFF ACT Node, Canberra, Australia Sent from my iPhone On 20 Feb 2018, at 3:43 am, Aebersold,Julia W. > wrote: We emphasize a very clean backside before processing is performed. Also, if processing has been performed prior to etching on the wafer then it can incur deformational stress that just makes it hard to sit on the chuck without an elevated leak up rate. We also change the chuck o-rings when the rate starts to climb and perform O2 chamber cleans on a regular basis. Cheers! Julia Aebersold Manager, Micro/Nano Technology Center University of Louisville Shumaker Research Building, Room 233 2210 South Brook Street Louisville, KY 40292 (502) 852-1572 http://louisville.edu/micronano/ From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Luciani, Vincent (Fed) Sent: Friday, February 16, 2018 3:49 PM To: labnetwork at mtl.mit.edu Subject: [labnetwork] Oxford ICP helium backside cooling performance Hello All, We have 2 Oxford Plasmalab 100 ICP etch tools that are heavily used. 100 mm wafers are the most popular. I am sure I discussed with many of you the trials and tribulations about these tools. My question is about a yur experiences and lessons learned with regard to keeping the helium leak rate from underneath the wafer under control. I am trying to get a general idea of what is typical and how we are doing compared to that. We have several users that utilize the cryonic etching capability of our tools so the helium cooling is very important. For those using the tool at -100 C, we find that 8 sccm is too high and users request repair. We generally try to keep the leak rate < 5 sccm at all time but find this difficult to do with the variety of substrates and etch recipes. We made some progress by ordering specially made quartz discs with a cutout for the wafer flat for better wafer positioning. I am happy to share the dwg if anyone would like it. What is your experience? What leak rate do you find tolerable and at what leak rate do you shut the tool down. Any tricks you can share? Thanks, Vince Vincent K. Luciani NanoFab Manager Center for Nanoscale Science and Technology National Institute of Standards and Technology 100 Bureau Drive, MS 6201 Gaithersburg, MD 20899-6200 USA +1-301-975-2886 _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://mtl.mit.edu/mailman/listinfo.cgi/labnetwork -------------- next part -------------- An HTML attachment was scrubbed... URL: From Vincent.Luciani at nist.gov Thu Feb 22 16:15:58 2018 From: Vincent.Luciani at nist.gov (Luciani, Vincent (Fed)) Date: Thu, 22 Feb 2018 21:15:58 +0000 Subject: [labnetwork] Helium leak rate on Oxford RIE Message-ID: Hello All, Thanks for all the great feedback about the backside helium leak rate on the Oxford tools. To sum up it sounds like most labs strive to keep it less than 10 sccm and 6 -12 sccm is a typical range. It is very helpful to see that what we observe is fairly typical. We have one process that etches at -100 C with very high RF and ICP power that requires < 5 sccm. We can get it there for this user but keeping it there is difficult. For those who asked for the drawings of our modified quartz plate, I will send that to you individually. I plan to invest in some mechanical design engineering effort to make these cooled chucks perform better. I'll share anything we come up with. Thanks again, Vince Vincent K. Luciani NanoFab Manager Center for Nanoscale Science and Technology National Institute of Standards and Technology 100 Bureau Drive, MS 6201 Gaithersburg, MD 20899-6200 USA +1-301-975-2886 -------------- next part -------------- An HTML attachment was scrubbed... URL: From spaolini at cns.fas.harvard.edu Thu Feb 22 18:14:59 2018 From: spaolini at cns.fas.harvard.edu (Paolini, Steven) Date: Thu, 22 Feb 2018 23:14:59 +0000 Subject: [labnetwork] Helium leak rate on Oxford RIE In-Reply-To: References: Message-ID: Hi Vince, Sorry for such a late response but I hadn't noticed anyone mentioning the pressure of the cavity behind the wafer. Assuming that your system has that capability, the flow of He should be judged by the backside pressure. As an example, we have many etching systems here with mechanical wafer clamps and we baseline them when new to flow X amount of He for a specified pressure (closed loop system). As you may expect, the flow of He increases as the backside pressure is called to increase. We use this baseline flow as criteria to either change a seal if applicable, clean the wafer backside or clean the chuck if necessary. We have gotten very good with our tool set to have a seal change or chuck clean at PM intervals. Oh yeah, beware of the photo users that neglect edge bead removal after coating, it can cause the wafer to stick to the chuck and when it begins to transfer out, the lift will "pop" it off the chuck and most certainly position it in a bad spot. Steve "Equipment Dood" Paolini Steve Paolini Principal Equipment Engineer Harvard University Center for Nanoscale Systems 11 Oxford St. Cambridge, MA 02138 617- 496- 9816 spaolini at cns.fas.harvard.edu www.cns.fas.harvard.edu From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Luciani, Vincent (Fed) Sent: Thursday, February 22, 2018 4:16 PM To: labnetwork at mtl.mit.edu Subject: [labnetwork] Helium leak rate on Oxford RIE Hello All, Thanks for all the great feedback about the backside helium leak rate on the Oxford tools. To sum up it sounds like most labs strive to keep it less than 10 sccm and 6 -12 sccm is a typical range. It is very helpful to see that what we observe is fairly typical. We have one process that etches at -100 C with very high RF and ICP power that requires < 5 sccm. We can get it there for this user but keeping it there is difficult. For those who asked for the drawings of our modified quartz plate, I will send that to you individually. I plan to invest in some mechanical design engineering effort to make these cooled chucks perform better. I'll share anything we come up with. Thanks again, Vince Vincent K. Luciani NanoFab Manager Center for Nanoscale Science and Technology National Institute of Standards and Technology 100 Bureau Drive, MS 6201 Gaithersburg, MD 20899-6200 USA +1-301-975-2886 -------------- next part -------------- An HTML attachment was scrubbed... URL: From RobertVandusen at cunet.carleton.ca Fri Feb 23 07:52:52 2018 From: RobertVandusen at cunet.carleton.ca (Robert Vandusen) Date: Fri, 23 Feb 2018 12:52:52 +0000 Subject: [labnetwork] Mann PG3000 pattern generator question Message-ID: Hi everyone. I was hoping to find someone who may have experience with the Mann PG1600 or PG3000 pattern generator mask making systems. In our Microfab we have 2 working David W. Mann pattern generators: a PG1600 and a PG3000. These units are still working fairly well, but we would like to try adjusting the lens focus to match up with different size plate holders. I know according to the manual it is a matter of adjusting the knurled vernier wheel at the top of the lens housing. I have tried this and there does not seem to be any movement. I did not want to force in case there is something else that needs to be loosened or lubricated first. I have tried reaching out to my former contacts from the former Mann company with no luck. Thanks in advance. Rob Robert Vandusen Microfabrication and FANSSI Cleanlab Facility Manager Electronics Department Carleton University room: 4184 Mackenzie Building 613-520-2600 ext 5761 Robert_vandusen at cunet.carleton.ca -------------- next part -------------- An HTML attachment was scrubbed... URL: From kjvowen at lnf.umich.edu Fri Feb 23 16:45:26 2018 From: kjvowen at lnf.umich.edu (Kevin Owen) Date: Fri, 23 Feb 2018 16:45:26 -0500 Subject: [labnetwork] Processing alternatives during extended etch tool downtime (LAM 9400) Message-ID: Happy Friday, everyone! We're having some controller issues with our LAM 9400SE and LAM has now extended us to a 6 week lead time on the board we *hope* will solve the problem, so in the meantime we are looking for alternative locations for some of our users to be able to continue their processing. The tool supports a plethora of processes, many of which we should be able to transfer in-house to other equipment, but there are some needs we won't be able to fill. While I don't have any specific requests yet (we only just notified the users of the extension of the downtime), I suspect the areas we will need support in will be mostly: - pieces, 100, 150 mm Cl/HBr processing (mainly poly-Si) - 100-150 mm Cl/BCl3 processing (III-V and III-nitride and maybe a few others) If your lab might be willing to help some of these users (either via remote processing or sending the user on-site), please let me know what equipment you have that would support these processes and any material/size/process restrictions you have for the tools. For reference, our tool configuration and approved materials are detailed on our wiki (LAM 9400 ). There are some additional materials that may be approved in certain situations (e.g. buried by PR or another material), but we will be working with each user individually to determine what process they need and what other materials are present on their samples in order to direct them appropriately. Thanks, Kevin -- Kevin Owen Senior Engineer in Research Operations Group, Lurie Nanofabrication Facility University of Michigan (734) 545-4014 -------------- next part -------------- An HTML attachment was scrubbed... URL: From codreanu at udel.edu Mon Feb 26 13:49:11 2018 From: codreanu at udel.edu (Iulian Codreanu) Date: Mon, 26 Feb 2018 13:49:11 -0500 Subject: [labnetwork] reputable vacuum pump re-builders in the NE Message-ID: <8e08f1f4-876a-d826-f013-313c174557ef@udel.edu> Dear Colleague, I am looking for reputable vacuum pump rebuilders in the Northeast. Could you recommend anyone? Thank you very much, Iulian -- iulian Codreanu, Ph.D. Director of Operations, UD NanoFab 163 ISE Lab 221 Academy Street Newark, DE 19716 302-831-2784 http://udnf.udel.edu From mweiler at andrew.cmu.edu Mon Feb 26 17:16:01 2018 From: mweiler at andrew.cmu.edu (Mark Weiler) Date: Mon, 26 Feb 2018 22:16:01 +0000 Subject: [labnetwork] reputable vacuum pump re-builders in the NE In-Reply-To: <8e08f1f4-876a-d826-f013-313c174557ef@udel.edu> References: <8e08f1f4-876a-d826-f013-313c174557ef@udel.edu> Message-ID: Turbo, Cryo or rough (dry or wet)? Best, Mark ________________________________________________________________ Mark Weiler Fab & Facilites Manager CMU Nanofabrication Facility Dept. of Electrical & Computer Engineering 5000 Forbes Avenue Pittsburgh, PA 15213 P: 412-268-2471 F: 412-268-4323 www.ece.cmu.edu [cid:2D2E01E3-CEC1-4F48-A845-224D8D7CED12 at wv.cc.cmu.edu] On Feb 26, 2018, at 1:49 PM, Iulian Codreanu > wrote: Dear Colleague, I am looking for reputable vacuum pump rebuilders in the Northeast. Could you recommend anyone? Thank you very much, Iulian -- iulian Codreanu, Ph.D. Director of Operations, UD NanoFab 163 ISE Lab 221 Academy Street Newark, DE 19716 302-831-2784 http://udnf.udel.edu _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://mtl.mit.edu/mailman/listinfo.cgi/labnetwork -------------- next part -------------- An HTML attachment was scrubbed... URL: -------------- next part -------------- A non-text attachment was scrubbed... Name: images.png Type: image/png Size: 720 bytes Desc: images.png URL: From michael.rooks at yale.edu Mon Feb 26 17:24:36 2018 From: michael.rooks at yale.edu (Michael Rooks) Date: Mon, 26 Feb 2018 17:24:36 -0500 Subject: [labnetwork] reputable vacuum pump re-builders in the NE In-Reply-To: <8e08f1f4-876a-d826-f013-313c174557ef@udel.edu> References: <8e08f1f4-876a-d826-f013-313c174557ef@udel.edu> Message-ID: <5A948924.9010805@yale.edu> We use Orange County Vacuum, aka Standard Vacuum: Richard Trivolis Orange County Vacuum 845 283-2800 Cell www.ocvacuum.com Representing Standard Vacuum Bohemia,NY. www.standardvacuum.com They are a good source for rebuilt roughing pumps. -------------------------------- Michael Rooks Yale Institute of Nanoscience and Quantum Engineering nano.yale.edu On 02/26/2018 01:49 PM, Iulian Codreanu wrote: > Dear Colleague, > > I am looking for reputable vacuum pump rebuilders in the Northeast. > Could you recommend anyone? > > Thank you very much, > > Iulian > -------------- next part -------------- An HTML attachment was scrubbed... URL: From cknollen at stanford.edu Tue Feb 27 12:58:20 2018 From: cknollen at stanford.edu (Clifford F Knollenberg) Date: Tue, 27 Feb 2018 17:58:20 +0000 Subject: [labnetwork] EBeam Lithography on Glass substrates In-Reply-To: <15343E46-7A29-4D8B-AE71-443F450E6D20@upenn.edu> References: <072A267E-4725-4880-BFCE-CB65EB1B4EB5@uiowa.edu> <1f37445b-cd3b-c5ed-c4be-e2e496b7873b@mit.edu> <5e7dd2b364944e80bda4f2c16fe6ae94@PGH-MSGMLT-03.andrew.ad.cmu.edu> <6C521A5E02323C4CB73135692FB72A8548FB46F4@SRV362.tudelft.net> <8c9fb7bce4e18cfd0cc2340edcff771a@mail.gmail.com> , <15343E46-7A29-4D8B-AE71-443F450E6D20@upenn.edu> Message-ID: The violet light you see in a plasma is going to be in the range of 380-450nm. As the reference below shows, PMMA absorption starts at 280nm and doesn't get really get going until 225nm. That's a pronounced energy difference. If you really want to get emission below 350nm you need a mercury bulb or an excimer laser. -Cliff Clifford Knollenberg Science & Engineering Associate Stanford Nano Shared Facilities (SNSF) Email: cknollen at stanford.edu Tel: 650-723-1675 ________________________________ From: labnetwork-bounces at mtl.mit.edu on behalf of Noah Clay Sent: Thursday, August 24, 2017 6:29 PM To: N . Shane Patrick Cc: labnetwork at mtl.mit.edu; Ryan Anderson Subject: Re: [labnetwork] EBeam Lithography on Glass substrates Maybe this was mentioned earlier, but PMMA is strongly absorbing below 220 - 225 nm. http://www.allresist.com/photorestist-other-resists-uv-patterning-of-pmma-resist/ [http://www.allresist.com/wp-content/themes/allresist_en/img/facebook-logo.jpg] Resist-Wiki: UV-patterning of PMMA resists - Allresist EN ... www.allresist.com PMMA resists can also be patterned using UV-lithography, but only at exposure wavelengths of 200 ? 270 nm (deep UV light). Sent from my iPhone On Aug 24, 2017, at 15:41, N . Shane Patrick > wrote: We use sputtered Au/Pd exclusively here as a charge dissipation layer and have not seen any adverse effects. Our system for this is a very basic tabletop coater system that runs on 120V and takes maybe 2 minutes of sputtering to get a sufficient coating for our cases. Perhaps power/duration are important to consider. N. Shane Patrick Research Engineer, Washington Nanofabrication Facility (WNF) National Nanotechnology Coordinated Infrastructure (NNCI) University of Washington Fluke Hall 132, Box 352143 (206) 221-1045 patricns at uw.edu http://www.wnf.washington.edu/ UW NNCI Washington Nanofabrication Facility www.wnf.washington.edu Nanofabrication Short Course We're pleased to offer a one-week survey course that introduces key nanofabrication techniques, tools and methods from March 19-23. On Aug 24, 2017, at 10:50 AM, Ryan Anderson > wrote: Hi all, We have also observed adverse effects on PMMA exposure (100kV) after sputter coating gold. Since then we have used thermal evaporation. Ryan Anderson UC San Diego, Nano3 -----Original Message----- From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Fouad Karouta Sent: Wednesday, August 23, 2017 4:15 PM To: Marc Zuiddam - TNW >; 'labnetwork at mtl.mit.edu' > Subject: Re: [labnetwork] EBeam Lithography on Glass substrates Dear Marc, Evaporating Au on PMMA or ZEP should be done in a thermal evaporator, an e-beam evaporator due to the electron beam would affect the resist. We also avoid sputtering for this application as the effect of Ar plasma (violet colour) can be unpredictable. Regards, Fouad -----Original Message----- From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Marc Zuiddam - TNW Sent: Wednesday, 23 August 2017 10:29 PM To: 'labnetwork at mtl.mit.edu' > Subject: Re: [labnetwork] EBeam Lithography on Glass substrates Dear people, I always have the idea that sputting/evaporating a thin Au layer on my sample is exposing the e-beam resist on my sample.. Do you also experience that? Regards, Marc Zuiddam -----Original Message----- From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Fouad Karouta Sent: woensdag 23 augustus 2017 1:42 To: Jugessur, Aju S; labnetwork at mtl.mit.edu Subject: Re: [labnetwork] EBeam Lithography on Glass substrates Hi Aju, Am echoing other voices: - We use 12 nm of Au mostly on top of PMMA/ZEP to do the EBL which we remove in a Ki/I2 solution. - Sometime we use Cr under resist layer as well when we need Cr for further processing. Regards, Fouad Karouta ************************************* Manager ANFF ACT Node Australian National Fabrication Facility Research School of Physics and Engineering L. Huxley Building (#56), Mills Road, Room 4.02 Australian National University ACT 0200, Canberra, Australia Tel: + 61 2 6125 7174 Mob: + 61 451 046 412 Email: fouad.karouta at anu.edu.au http://anff-act.anu.edu.au/ [http://anff-act.anu.edu.au/Images/sidebar/ANFF_network.jpg] ANFF ACT & WA Nodes - Home anff-act.anu.edu.au Welcome to ANFF ACT & WA Nodes . Our Mission "To offer a state-of-the-art facility and processing capabilities open to all scientists and researchers in Australia and ... -----Original Message----- From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Lino Eugene Sent: Tuesday, 22 August 2017 11:49 PM To: labnetwork at mtl.mit.edu Cc: Steven Wei > Subject: Re: [labnetwork] EBeam Lithography on Glass substrates Hi Aju, We have a coop student who has worked on different anti-charging materials: PEDOT:PSS, Electra 92 and sputtered Al. We had also adhesion and uniformity issues with PEDOT:PSS from Sigma-Aldrich. The solution was filtered and Triton X-100 was added and but no noticeable improvement. I was told that surface treatment with SurPass 3000 improves adhesion but we haven't tried this yet. Moreover, PEDOT:PSS cross-links under certain conditions and then the layer cannot be removed with water. 10-20 nm of sputtered Al should work well . The resistivity of 5 nm Al is expected to be high because of surface electron scattering (electron mean free path in Al at room temperature is ~19nm) and oxidation. We use MF-319 at room temperature or 40 degC to remove the layer. Electra 92 from AllResist is easy to work with as it can be removed with DI water after EBL and gives pretty good results on PMMA and on ZEP520A. Surface treatment on HSQ is needed, so far treatment with IPA gives good results. Also, the price is reasonable compared to ESpacer and AquaSave. Best, Lino Eugene, Ph.D., Jr. Eng. Micro/nanofabrication process engineer Quantum NanoFab University of Waterloo 200 University Avenue West Waterloo, ON, Canada N2L 3G1 Ph: +1 519-888-4567 #37788 Cell: +1 226-929-1685 Website: https://fab.qnc.uwaterloo.ca/ -----Original Message----- From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Matthew Moneck Sent: August 21, 2017 21:09 To: Mark K Mondol >; labnetwork at mtl.mit.edu Subject: Re: [labnetwork] EBeam Lithography on Glass substrates Hi Aju, We have commonly used Al as a conductive layer on top of PMMA on glass (removal is typically done with minimal damage by using dilute AZ400K photoresist developer). However, 5nm seems to be on the thin side. Al can form native oxide that is up to 3-4nm thick. Therefore, I would confirm the answer to Mark's question of whether or not the 5nm Al layer is conductive. We typically sputter deposit films that are 10-20nm thick for our applications. Best Regards, Matt -- Matthew T. Moneck, Ph.D. Executive Manager, Carnegie Mellon Nanofabrication Facility Electrical and Computer Engineering | Carnegie Mellon University 5000 Forbes Ave., Pittsburgh, PA 15213-3890 T: 412.268.5430 F: 412.268.3497 www.ece.cmu.edu Electrical and Computer Engineering at Carnegie Mellon ... www.ece.cmu.edu ECE is a department of the Carnegie Institute of Technology at Carnegie Mellon University. nanofab.ece.cmu.edu Nanofabrication Laboratory at Carnegie Mellon University nanofab.ece.cmu.edu Nanofabrication Laboratory at Carnegie Mellon University. A lab of the Electrical and Computer Engineering Department. -----Original Message----- From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Mark K Mondol Sent: Monday, August 21, 2017 5:04 PM To: labnetwork at mtl.mit.edu Subject: Re: [labnetwork] EBeam Lithography on Glass substrates Aju: 1. Be 100% certain the layer is conductive and connected to ground in the tool. 2. Every time they write on glass, do the same exposure on Si, if the problem shows up on both Si and glass the issue is not the insulating substrate. 3. Al etch can damage PMMA; not always in a repeatable way. Does your process include etching the Al (I have found Transene CR-7 chrome etch to be compatible with PMMA and ZEP, so usually use Cr not Al as the conductive layer). Regards, Mark K MOndol -- Mark K Mondol Assistant Director NanoStructures Laboratory And Facility Manager Scanning Electron Beam Lithography Facility Bldg 36 Room 229 www.rle.mit.edu/sebl RLE :: SEBL at RLE :: MIT's Scanning-Electron-Beam ... www.rle.mit.edu T he scanning-electron-beam lithography (SEBL) facility enables the writing of patterns of arbitrary geometries with minimum features as fine as 17 nm. mondol at mit.edu office - 617-253-9617 cell - 617-224-8756 _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://www-mtl.mit.edu/mailman/listinfo.cgi/labnetwork _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://www-mtl.mit.edu/mailman/listinfo.cgi/labnetwork _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://www-mtl.mit.edu/mailman/listinfo.cgi/labnetwork _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://www-mtl.mit.edu/mailman/listinfo.cgi/labnetwork _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://www-mtl.mit.edu/mailman/listinfo.cgi/labnetwork _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://www-mtl.mit.edu/mailman/listinfo.cgi/labnetwork _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://www-mtl.mit.edu/mailman/listinfo.cgi/labnetwork _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://www-mtl.mit.edu/mailman/listinfo.cgi/labnetwork -------------- next part -------------- An HTML attachment was scrubbed... URL: From rdevito at draper.com Tue Feb 27 13:04:34 2018 From: rdevito at draper.com (DeVito, Richard) Date: Tue, 27 Feb 2018 18:04:34 +0000 Subject: [labnetwork] reputable vacuum pump re-builders in the NE In-Reply-To: <8e08f1f4-876a-d826-f013-313c174557ef@udel.edu> References: <8e08f1f4-876a-d826-f013-313c174557ef@udel.edu> Message-ID: <00421bcdc63a4714916ab275f1aad5cd@draper.com> Iulian we do a lot of work with Ebara...they rebuild other as well as their pumps-quality work Rich D Rich DeVito Principle Member Technical Staff Group Leader Microfabrication Lab Draper 555 Technology Square, Cambridge, MA 02139 Phone: 617-258-3819 www.draper.com -----Original Message----- From: labnetwork-bounces at mtl.mit.edu [mailto:labnetwork-bounces at mtl.mit.edu] On Behalf Of Iulian Codreanu Sent: Monday, February 26, 2018 1:49 PM To: Fab Network Subject: [labnetwork] reputable vacuum pump re-builders in the NE Dear Colleague, I am looking for reputable vacuum pump rebuilders in the Northeast. Could you recommend anyone? Thank you very much, Iulian -- iulian Codreanu, Ph.D. Director of Operations, UD NanoFab 163 ISE Lab 221 Academy Street Newark, DE 19716 302-831-2784 http://udnf.udel.edu _______________________________________________ labnetwork mailing list labnetwork at mtl.mit.edu https://mtl.mit.edu/mailman/listinfo.cgi/labnetwork ________________________________ Notice: This email and any attachments may contain proprietary (Draper non-public) and/or export-controlled information of Draper. If you are not the intended recipient of this email, please immediately notify the sender by replying to this email and immediately destroy all copies of this email. ________________________________ From jpalmer at Princeton.EDU Tue Feb 27 15:15:57 2018 From: jpalmer at Princeton.EDU (Joseph E. Palmer) Date: Tue, 27 Feb 2018 15:15:57 -0500 Subject: [labnetwork] reputable vacuum pump re-builders in the NE In-Reply-To: <8e08f1f4-876a-d826-f013-313c174557ef@udel.edu> References: <8e08f1f4-876a-d826-f013-313c174557ef@udel.edu> Message-ID: I use PolVac, and have been very happy with them. http://www.polvac.com/ Regards, Joe Palmer On 2/26/2018 1:49 PM, Iulian Codreanu wrote: > Dear Colleague, > > I am looking for reputable vacuum pump rebuilders in the Northeast. > Could you recommend anyone? > > Thank you very much, > > Iulian > From nadia.court at sydney.edu.au Tue Feb 27 23:24:14 2018 From: nadia.court at sydney.edu.au (Nadia Court) Date: Wed, 28 Feb 2018 04:24:14 +0000 Subject: [labnetwork] Micro- and Nano-fab job opportunities in Sydney Message-ID: Dear All, The University of Sydney is continuing to grow it?s micro and nanofabrication facility and we are looking for more skilled staff to join our team. This is a great opportunity to contribute to the building of this new facility in a purpose-built state-of-the-art cleanroom in the Sydney Nanoscience Hub, the home of the University of Sydney Nano Institute. The facility is one of the University?s Core Research Facilities, and part of the Australian National Fabrication Facility network. It?s an exciting time as the Hub and cleanroom are very new and about a third of the equipment is installed and running, with new tools arriving regularly. We are currently recruiting into two positions, and applications for both close on Sunday 11 March 2018. Cleanroom Technical Officer Process Engineer: Optical Lithography Unfortunately, we are unable to provide visa sponsorship for this position. However, if you have the right to work in Australia through other means we encourage you to apply. Kind Regards, Nadia Dr Nadia Court Facility and Program Manager | Research & Prototype Foundry Core Research Facilities | Research Portfolio The University of Sydney Rm 4025, Sydney Nanoscience Hub A31 | The University of Sydney | NSW | 2006 T +61 2 8627 8671 E nadia.court at sydney.edu.au | W Sydney's Core Research Facilities ANFF OptoFab: www.anff.org.au CRICOS 00026A This email plus any attachments to it are confidential. Any unauthorised use is strictly prohibited. If you receive this email in error, please delete it and any attachments. Please think of our environment and only print this e-mail if necessary. -------------- next part -------------- An HTML attachment was scrubbed... URL: